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Incorporation of an allene unit into alpha-pinene: Generation of the cyclic allene 2,7,7-trimethylbicyclo[4.1.]octa-2,3-diene and its dimerization

Azizoğlu, Akın; Özen, Recep; Hökelek, Tuncer; Balcı, Metin (Amer Chemical Soc, 2004)

The reaction of etheral methyllithium with 3,3-dibromo-2,7,7-trimethyl-tricyclo[4.1.1.0.(2,4)] octane (2) was investigated. The generated carbene 12 undergoes intramolecular C-H insertion to provide the tetracyclic hydrocarbon ...