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dc.contributor.authorBülbül, Berna
dc.contributor.authorBeyaz, Seda
dc.date.accessioned2021-04-02T06:54:42Z
dc.date.available2021-04-02T06:54:42Z
dc.date.issued2020en_US
dc.identifier.issn2083-134X
dc.identifier.urihttps://doi.org/10.2478/msp-2019-0092
dc.identifier.urihttps://hdl.handle.net/20.500.12462/11377
dc.description.abstractAmorphous lead metaborate (Pb(BO2)(2)center dot H2O) nanostructures were synthesized by a simpl and cost-effective synthesis method which is based on precipitation of lead ions using boric acid/sodium hydroxide buffer (pH 9.2) in the presence of polyethylene glycol (PEG). Scanning electron microscopy images showed that the average particle size is 30 +/- 9 nm and the particle shape is mostly spherical. The chemical formulation of Pb(BO2)(2)center dot H2O was confirmed by infrared spectroscopy, inductively coupled plasma and thermal gravimetric analysis (TGA). The percentage of PEG molecules on the particle surface equal to 2.5 % was determined by TGA. Optical reflectance measurement was performed by UV-Vis spectroscopy. Based on the Kubelka-Munk function, it was calculated that the Pb(BO2)(2)center dot H2O nanostructures have a direct band gap of 4.6 eV.en_US
dc.language.isoengen_US
dc.publisherSciendoen_US
dc.relation.isversionof10.2478/msp-2019-0092en_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.rightsAttribution-NonCommercial-NoDerivs 3.0 United States*
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/3.0/us/*
dc.subjectLead Metaborateen_US
dc.subjectNanomaterialsen_US
dc.subjectChemical Synthesisen_US
dc.titleDeveloping of buffer-precipitation method for lead metaborate (Pb(BO2)(2)center dot H2O) nanostructuresen_US
dc.typearticleen_US
dc.relation.journalMaterials Science- Polanden_US
dc.contributor.departmentFen Edebiyat Fakültesien_US
dc.contributor.authorID0000-0002-0508-4878en_US
dc.contributor.authorID0000-0002-6422-675Xen_US
dc.identifier.volume38en_US
dc.identifier.issue1en_US
dc.identifier.startpage138en_US
dc.identifier.endpage142en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US


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